Question

In: Chemistry

QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 5) Would it have been okay to...

QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules)

5) Would it have been okay to use gravity filtration rather than suction filtration for the recrystallized product? WHY or WHY not?

Solutions

Expert Solution

Gravity filtration is generally used in the case to remove solid impurities and particals present in liquid. It is not efficient in the case to the liquid impurities from the solid particles. It is not preferrable to filter crystallized solid substance from liquid under hot conditions. It is a slow process takes long time. While filtering under hot conditions of a recrystallized solid substance from liquid solidification takes place. So that gravity filtration is not suitable those processes

Suction filtration is used in the case of liquid impurities along with solid substance. It is faster and more efficient in the case of recrystallized product.

5) Answer

In preparation of m-dinitro benzene there are many impurities present (0-dinitro benzene and p-dinitro benzene).

In recrystallization process to remove all the impurities efficientyl from the solid substance to get pure compound.

The filtration must be performed under hot conditions. slow process is not prefferable.

Gravity filtration is less efficient.


Related Solutions

QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 1) what effect would the use of...
QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 1) what effect would the use of concentrated nitric acid in place of the fuming nitric acid have on the yield on m-dinitrobenzene? Explain Fully. 2) During the washing of the "crude" Product, the filtrate was checked with pH paper as it dripped from the funnel. Why was this done rather then check the filtrate that collected in the suction flask? Explain Fully. 3) give the name and formula of the...
QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 3) give the name and formula of...
QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 3) give the name and formula of the principal organic impurity removed during the recrystallization of the dinitrobenzene. How can you account for the presence of this impurity?
QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 7) Explain why the meta product is...
QUESTIONS FOR m-Dinitrobenzene lab (Nitration of the aromatic molecules) 7) Explain why the meta product is formed and not the ortho or para.
Consider the following assets: Bad Okay Good Market M -5% 5% 15% Asset X -2% -3%...
Consider the following assets: Bad Okay Good Market M -5% 5% 15% Asset X -2% -3% 25% Asset Y -4% -6% 30% Assume each scenario is equally likely Do the following: a.) Compute the market betas for assets X and Y. b.) Compute the correlations for X and Y with M. c.) Assume you were holding only M. You now are selling 10% of your M portfolio to replace it with 10% of either X or Y. Would an M...
Some anthocyanins have sugar molecules attached to both the 3 and 5 position. These molecules are...
Some anthocyanins have sugar molecules attached to both the 3 and 5 position. These molecules are called diglycosides. Assuming that sugar increases the polarity (hydrophilicity) of the anthocyanin molecule, would a diglycoside migrate further or less than a monoglycoside on TLC?
In lab this semester, we have examined several cellular molecules and activities including, but not limited...
In lab this semester, we have examined several cellular molecules and activities including, but not limited to, cyclosis in Elodea, Protein concentration in various food sources, bovine serum albumin and the relationship between protein concentration and absorbance, Betacyanin and membrane permeability, B-galactosidase and enzyme function, yeast cell growth, and RNA production in cells. Describe how one of more of the databases/programs utilized in this lab exercise (pBLAST, PDB, DeepLoc, KEGG) could be used to gain information about one of these...
In the Force lab, we use a small lab car with mass m=5 Kg, the experiment...
In the Force lab, we use a small lab car with mass m=5 Kg, the experiment is on a horizontal table, on the car is acting a pulling force F= 20 N and the kinetic friction force Fr is acting as well. The car initially is at rest, and take 6.0 seconds to reach the velocity of 8.5 m/s. a)       Calculate the magnitude of the friction force Fr acting on the car? b)      We remove the pulling force when the...
REQUIREMENT 2, 5 & 9 Okay, I have a case study I need to complete by...
REQUIREMENT 2, 5 & 9 Okay, I have a case study I need to complete by the end of this week but I am stuck. Plus, I need to make sure that I am doing this correctly. It is a layered challenge. I will have to send the study in pieces because I could not attach the actual document.    This Sheet will be used for Requirements 2, 5, and 9.                              Requirement #2:      ...
Data Tables and Post-Lab Assessment Lab Questions 1.     Transcribe the following DNA sequence: Hb A: 5’...
Data Tables and Post-Lab Assessment Lab Questions 1.     Transcribe the following DNA sequence: Hb A: 5’ AGT AAC GGC AGA CTT CTC CTC AGG AGT CAG GTG CAC CAT 3’ 3'UCA UUG CCG UCU GAA GAG GAG UCC UCA GUC CAC GUG GUA 5' 2.     Translate your new RNA sequence using the genetic code. Remember that when determining your amino acid sequence, the RNA sequence is read from 5’ to 3’. val- val -his- val- ser -ser- glu- glu- ser-ser-...
You will have been given one of the molecules depicted in the introduction as your unknown...
You will have been given one of the molecules depicted in the introduction as your unknown (anthracene, naphtalene,fluorene, p-dichlorobenzene) Which do you believe it is? Base your choice on the experimental molar mass you calculated (123g/mol)from your data, and comment on how certain you are of your identification.
ADVERTISEMENT
ADVERTISEMENT
ADVERTISEMENT