In: Chemistry
Calculate % yield of triphenylmethanol (crude and pure)
Remember it is a two step calculations, so you should obtain the following to aid in the calculations: the mass of first reagent, mass of second reagent (including HCl – Vol & Density), and moles of both reagents (for each procedure). Then set up a Balanced Stoichiometric Equation, determine the molar ratio, determine limiting reagent and compute the theoretical yield.
These are the values:
Bromobenzene + Magnesium -->
Phenylmagnesium Bromide
Phenylmagnesium Bromide + Benzophenone ---> Triphenylmethanol + Magnesium Bromide Hydroxide
0.1538g of Mg 0.9mL Bromo/Ether solution 1.0910 benzophenone +
2mL ether —-> 0.349g
6mL of 6M HCl 2mL diethyl ether 0.301g
triphenylmethanol (recrystalized and weighed 0.201 g
triphenylmethanol)
You did mention which one is benzophenone weight . I took 0.349 gm as benzophenone weight