Will the product of this reaction (9-fluorenone to 9-fluorenol) differ if LAH is used instead of...

Will the product of this reaction (9-fluorenone to 9-fluorenol) differ if LAH is used instead of sodium borohydride.?

Expert Solution

queen_honey_blossom answered 2 years ago

In regards to the synthesis of 9-fluorenone via sodium hypochlorite oxidation of 9-fluorenol (9-Fluorenol -> 9-fluorenone)...

In regards to the synthesis of 9-fluorenone via sodium hypochlorite oxidation of 9-fluorenol (9-Fluorenol -> 9-fluorenone) lab answer the following question: What would happen if this oxidation were carried out with 9-methyl-9-fluorenol?

You will apply the oxidation reaction to 9-fluorenol to obtain 9-fluorenone: 1. Describe the role of...

You will apply the oxidation reaction to 9-fluorenol to obtain 9-fluorenone: 1. Describe the role of each chemical in this reaction. Reagent Role 9-fluorenol H2CrO4 acetone ether hexanes 2. What is the actual oxidizing agent in this experiment? What is it reduced to? 3.After all of the 9-flurenol has undergone reaction, it is necessary to destroy the excess oxidizing agent in the reaction mixture. How is this done? 4. Imagine that you will monitor the reaction progress by TLC. Will...

Can you please explain the oxidation reaction of 9-fluorenol to 9-fluorenone using sodium hypochlorite, preferably a...

Can you please explain the oxidation reaction of 9-fluorenol to 9-fluorenone using sodium hypochlorite, preferably a detailed explanation of everything that is happening.

What are some possible sources of error in the oxidation of 9-fluorenol to 9-fluorenone with sodium...

What are some possible sources of error in the oxidation of 9-fluorenol to 9-fluorenone with sodium hypochlorite?

A sample of 9-fluorenone is contaminated with an impurity that is insoluble in ethanol. 9-Fluorenone is...

A sample of 9-fluorenone is contaminated with an impurity that is insoluble in ethanol. 9-Fluorenone is a bright yellow solid that dissolves in hot ethanol. Use this information to design the experimental procedure to purify 9-fluorenone. Describe the procedure.

Draw the confirmation of 9-fluorenone

What is the mechanism for separating 9-fluorenone and a carboxylic acid in mixture? We are using...

What is the mechanism for separating 9-fluorenone and a carboxylic acid in mixture? We are using a separatory funnel and adding the mixture of 9-fluorenone and a carboxylic acid to it. I need to know the mechanism of how they will separate into an aqueous and an organic layer.

1.1g of 9-fluorenol mixed with 11.1mL of hot methanol .11g of NaBH4 was then added. 3M...

1.1g of 9-fluorenol mixed with 11.1mL of hot methanol .11g of NaBH4 was then added. 3M of sulfuric acid was then added to the mixture, resulting in the formation of a solid. The mixture was then heated until the solid that formed upon the acid addition was dissolved in the solvent(methanol), and then cooled to room temperature. 9-fluorenol NMR: I've provided two sets of NMR's. The theoretical vs. the experimental. In the theoretical I understand all the shifts except for...

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9-fluorenol NMR: I've provided two sets of NMR's. The theoretical vs. the experimental. In the theoretical...

9-fluorenol NMR: I've provided two sets of NMR's. The theoretical vs. the experimental. In the theoretical I understand all the shifts except for the 2.06, representative of the H alpha to the OH group. Methine protons usually have a shift around 1.7ppm and protons alpha to an (OH) are deshieled adding +2.5ppm, according to my textbook, which would make me think that the actual shift be 4.2ppm. Why is this not the case? Could I be mistaking this nuclei for...

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