1. draw a mechanism for the conversion of methoxybenzyl alcohol
to methoxybenzaldehyde.
2.The ethyl acetate layer was extracted with 0.2M NaOH to remove
traces of methoxybenzoic acid that result from additional oxidation
of the aldehyde to the carboxylic acid. Explain how crystals of methoxybenzoic acid
could be isolated from the NaOH solution.
3. Explain how TLC could be used
to monitor the reduction of methoxybenzaldehyde to methoxybenzyl
alcohol using NaBH4 as a reducing agent.
Figure out the RI mixture mole fraction of ethyl acetate and butyl acetate with these numbers: A- Pure ethyl acetate: 1.3715 B-Pure butyl acetate: 1.3945 Fraction 1: 1.3715 Fraction 2: 1.384 and fraction 3: 1.395 all at a temperature of 20 degrees.
the formula is: RI mixture= Xa (RI pure A) + Xb (RI pure B).
2. Calculate the theoretical yield (g) of Zyban
hydrochloride
3. Write out the mechanism for the a-bromination of 1
(m-chloropropiophenone).
4. Step 2 is a substitution of bromine by t-butylamine. What
type of substitution is occurring: SN1 or SN2 Explain based on the
reaction’s substrate and solvent.
5. The reaction mixture from the substitution step 2 is
extracted with diethylether to isolate the product. State layer
(organic or aqueous) in which each of the following compounds will
be present in...
How do I find the theoretical yield for ethyl acetate? Started
with 5 mL of an unknown alcohol and added approximately 7 mL of
glacial acetic acid, then added 1 mL of concentrated sulfuric acid.
We then refluxed the reaction for 65 minutes.
What is the mechanism for separating 9-fluorenone and a
carboxylic acid in mixture? We are using a separatory funnel and
adding the mixture of 9-fluorenone and a carboxylic acid to it. I
need to know the mechanism of how they will separate into an
aqueous and an organic layer.
A mixture is 11 mol% ethanol, 79 mol% ethyl acetate (C4H8O2) and
10 mol% acetic acid (C2H4O2).
(a) Calculate the mass fraction of ethanol in this
three-component mixture.
(b) What is the average molecular weight of the three-component
mixture?
(c) What would be the mass (kg) of the three-component mixture
such that the mixture contains 24 kmol of ethyl acetate?
(d) A stream of the three-component mixture enters a mixing drum
at 78 kg/min. For a basis of 78 kg/min,...
A mixture of 4-methylphenol and 4-methylcyclohexanol was run on
a TLC plate using 3:1 hexane:ethyl acetate as the eluent. Only one
spot was seen using a UV lamp. Does this mean that both spots have
the same Rf or is there another explanation? How might
you solve this problem?